Synthesis and X-ray diffraction data for dibromo-dioxo-(1,10- phenanthroline-N,N′)-molybdenum(VI) (C12H8N2MoBr2O2)

Camargo, H. A.Henao, J. A.Castellanos, N. J.2019-12-042019-12-042016-02-17http://hdl.handle.net/11634/20112The dibromo-dioxo-(1,10-phenanthroline-N,N′)-molybdenum(VI) complex (C12H8N2MoBr2O2) was prepared from molybdic acid and 1,10-phenanthroline using hydrobromic acid as solvent. The molybdenum complex solid was separated by filtration and washed with ethyl ether. The X-ray powder diffraction pattern for the title compound was analyzed and found to crystallizes in monoclinic system, space group P21/c (No14) with refined unit-cell parameters a = 12.036 (1), b = 9.819 (1), c = 12.671 (2) Å, and β = 110.44° (1). The volume of the unit cell is V = 1403.2 (3) Å3.application/pdfAtribución-NoComercial-CompartirIgual 2.5 Colombiahttp://creativecommons.org/licenses/by-nc-sa/2.5/co/Synthesis and X-ray diffraction data for dibromo-dioxo-(1,10- phenanthroline-N,N′)-molybdenum(VI) (C12H8N2MoBr2O2)Dioxomolybdenum complexX-ray powder diffractionOxygen atom transferhttps://doi.org/10.1017/S0885715615000949Generación de Nuevo Conocimiento: Artículos publicados en revistas especializadas - Electrónicos