Obtaining nettle extracts (Urtica dioica L) by means of hydrocavitation

Vista sencilla de ítem
dc.contributor.advisorMalagón Romero, Dionisio Humberto
dc.contributor.authorAguirre Dúran, Esteban Felipe
dc.contributor.corporatenameUniversidad Santo Tomásspa
dc.contributor.cvlachttp://scienti.colciencias.gov.co:8081/cvlac/visualizador/generarCurriculoCv.do?cod_rh=0000167061
dc.contributor.googlescholarhttps://scholar.google.es/citations?user=b0ldFjcAAAAJ&hl=es
dc.contributor.orcidhttps://orcid.org/0000-0003-2890-2180
dc.date.accessioned2021-07-22T20:03:01Z
dc.date.available2021-07-22T20:03:01Z
dc.date.issued2021-06-07
dc.descriptionLa ortiga (Urtica dioica L.) se considera una gran fuente de metabolitos secundarios de interés comercial y la extracción de este tipo de metabolitos es importante para la viabilidad y escalado del proceso. Se han evaluado diferentes alternativas, incluida la extracción Soxhlet y el uso de fluidos supercríticos, principalmente a escala de laboratorio. Como enfoque innovador, la hidrocavitación ha surgido como una alternativa eficiente para extraer principios de plantas a bajas temperaturas y tiempos operativos cortos. Este trabajo presenta la extracción experimental de ß-caroteno de ortiga mediante hidrocavitación. Se utilizó etanol como disolvente a diferentes concentraciones (100%, 90%, 80% y 60%) y dos proporciones p / v soluto / disolvente (1:30 y 2:30). Se determinó la concentración de clorofila A, B, clorofilas totales (A + B), carotenos y ß-carotenos. La mejor concentración de ß-carotenos se obtuvo a razón soluto / disolvente 2:30 con etanol al 100% y un tiempo de operación de 2 minutos, correspondiente a 153,975 mg ß-carotenos / kg, con un consumo de energía de 0,7698 kJ / mg ß -caroteno extraído. Los resultados avalan la viabilidad del uso de la hidrocavitación para la obtención rápida y eficiente de extractos de ortiga a escala piloto y abren la posibilidad para el diseño de procesos a escala industrial.spa
dc.description.abstractAbstract- Stinging nettle (Urtica dioica L.) is considered a great source of secondary metabolites of commercial interest and the extraction of this kind of metabolites is important for the process viability and scale-up. Different alternatives have been evaluated, including Soxhlet extraction and the use of super critic fluids, mainly on laboratory scale. As an innovative approach, hydro-cavitation has emerged as an efficient alternative for extracting principles from plants at low temperatures and short operational times. This work presents the experimental extraction of ß-carotene from Stinging nettle employing hydro-cavitation. Ethanol was used as solvent at different concentrations (100%, 90%, 80% and 60%) and two w/v solute/solvent ratio (1:30 and 2:30). The concentration of chlorophyll A, B, total chlorophylls (A+B), carotenes, and ß-carotenes were determined. The best concentration of ß-carotenes was obtained at 2:30 solute/solvent ratio with ethanol at 100% and an operational time of 2 minutes, corresponding to 153.975 mg ß-carotenes/ kg, with a power consumption of 0.7698 kJ/mg ß-carotene extracted. The results support the viability of the use of hydro-cavitation for the rapid and efficient obtaining of Stinging nettle extracts on a pilot scale and open the possibility for the design of processes on an industrial scale.spa
dc.description.degreelevelPregradospa
dc.description.degreenameIngeniero Mecánicospa
dc.description.domainhttp://unidadinvestigacion.usta.edu.cospa
dc.format.mimetypeapplication/pdf
dc.identifier.citationA. D. E. Felipe, N. Galeano, G. Astrid, and M. Dionisio, “Obtaining nettle extracts ( Urtica dioica L ) by means of hydrocavitation.”retroexcavadoras [Trabajo de Pregrado Ingeniería Mecanica]. Repositorio institucional.spa
dc.identifier.instnameinstname:Universidad Santo Tomásspa
dc.identifier.reponamereponame:Repositorio Institucional Universidad Santo Tomásspa
dc.identifier.repourlrepourl:https://repository.usta.edu.cospa
dc.identifier.urihttp://hdl.handle.net/11634/34996
dc.language.isospa
dc.publisherUniversidad Santo Tomásspa
dc.publisher.branchCRAI-USTA Bogotáspa
dc.publisher.facultyFacultad de Ingeniería Mecánicaspa
dc.publisher.programPregrado Ingeniería Mecánicaspa
dc.relation.referencesD. Viboral, E. Retiro, and E. Santuario, “Medicinal plants used in some townships of municipalities in the high plainish,” vol. 33, no. 95, pp. 219–250, 2011.spa
dc.relation.referencesD. Orcic et al., “Quantitative determination of plant phenolics in Urtica dioica extracts by high-performance liquid chromatography coupled with tandem mass spectrometric detection,” Food Chem., vol. 143, pp. 48–53, 2014.spa
dc.relation.referencesC. Proestos, I. S. Boziaris, G. J. E. Nychas, and M. Komaitis, “Analysis of flavonoids and phenolic acids in Greek aromatic plants: Investigation of their antioxidant capacity and antimicrobial activity,” Food Chem., vol. 95, no. 4, pp. 664–671, 2006.spa
dc.relation.referencesR. Dhouibi et al., “Screening of pharmacological uses of Urtica dioica and others benefits,” Prog. Biophys. Mol. Biol., vol. 150, pp. 67–77, 2020.spa
dc.relation.referencesS. Otles and B. Yalcin, “Phenolic compounds analysis of root, stalk, and leaves of nettle,” Sci. World J., vol. 2012, 2012.spa
dc.relation.referencesR. Upton, “Stinging nettles leaf (Urtica dioica L.): Extraordinary vegetable medicine,” J. Herb. Med., 2013.spa
dc.relation.referencesN. A. Salih, “Effect of nettle (Urtica dioica) extract on gentamicin induced nephrotoxicity in male rabbits,” Asian Pac. J. Trop. Biomed., 2015.spa
dc.relation.referencesAhmed A. Abdeltawab, “Evaluation of the chemical composition and element analysis of Urtica dioica,” African J. Pharm. Pharmacol., vol. 6, no. 21, pp. 1555–1558, 2012.spa
dc.relation.referencesS. Đurović et al., “Chemical composition of stinging nettle leaves obtained by different analytical approaches,” J. Funct. Foods, vol. 32, pp. 18–26, 2017.spa
dc.relation.referencesS. Polat, “An in vitro evaluation of the effects of Urtica dioica and Fructus Urtica Piluliferae extracts on the crystallization of calcium oxalate,” J. Cryst. Growth, vol. 522, no. April, pp. 92–102, 2019.spa
dc.relation.referencesR. Kargozar, R. Salari, L. Jarahi, M. Yousefi, and S. Azam, “Complementary Therapies in Medicine Urtica dioica in comparison with placebo and acupuncture : A new possibility for menopausal hot flashes : A randomized clinical trial,” Complement. Ther. Med., vol. 44, no. January, pp. 166–173, 2019.spa
dc.relation.referencesB. Mansoori et al., “ScienceDirect Urtica dioica extract suppresses miR-21 and metastasis-related genes in breast cancer,” Biomed. Pharmacother., vol. 93, pp. 95–102, 2017.spa
dc.relation.referencesC. Bourgeois et al., “L’ortie (Urtica dioica L.), une source de produits antioxidants et phytochimiques anti-âge pour des applications en cosmétique,” Comptes Rendus Chim., vol. 19, no. 9, pp. 1090–1100, 2016.spa
dc.relation.referencesM. K. Akalin, S. Karagöz, and M. Akyüz, “Application of response surface methodology to extract yields from stinging nettle under supercritical ethanol conditions,” J. Supercrit. Fluids, 2013.spa
dc.relation.referencesN. Di Virgilio, E. G. Papazoglou, Z. Jankauskiene, S. Di Lonardo, M. Praczyk, and K. Wielgusz, “The potential of stinging nettle (Urtica dioica L.) as a crop with multiple uses,” Ind. Crops Prod., 2015.spa
dc.relation.referencesC. C. XU, B. WANG, Y. Q. PU, J. S. TAO, and T. ZHANG, “Advances in extraction and analysis of phenolic compounds from plant materials,” Chin. J. Nat. Med., vol. 15, no. 10, pp. 721–731, 2017.spa
dc.relation.referencesU. J. Vajić et al., “Optimization of extraction of stinging nettle leaf phenolic compounds using response surface methodology,” Ind. Crops Prod., 2015.spa
dc.relation.referencesT. T. Shonte, K. G. Duodu, and H. L. de Kock, “Effect of drying methods on chemical composition and antioxidant activity of underutilized stinging nettle leaves,” Heliyon, vol. 6, no. 5, 2020.spa
dc.relation.referencesM. Chaijan, K. Srirattanachot, M. Nisoa, L. Z. Cheong, and W. Panpipat, “Role of antioxidants on physicochemical properties and in vitro bioaccessibility of β-carotene loaded nanoemulsion under thermal and cold plasma discharge accelerated tests,” Food Chem., vol. 339, no. September 2020, p. 128157, 2021.spa
dc.relation.referencesM. A. T. Phan, M. Bucknall, and J. Arcot, “Interactive effects of β-carotene and anthocyanins on cellular uptake, antioxidant activity and anti-inflammatory activity in vitro and ex vivo,” J. Funct. Foods, vol. 45, no. February, pp. 129–137, 2018.spa
dc.relation.referencesC. Ba et al., “Effects of environmental stresses on physiochemical stability of β-carotene in zein-carboxymethyl chitosan-tea polyphenols ternary delivery system,” Food Chem., vol. 311, p. 125878, 2020.spa
dc.relation.referencesN. Y. Lee, Y. Kim, Y. S. Kim, J. H. Shin, L. P. Rubin, and Y. Kim, “β-Carotene exerts anti-colon cancer effects by regulating M2 macrophages and activated fibroblasts,” J. Nutr. Biochem., vol. 82, p. 108402, 2020.spa
dc.relation.referencesU. Blume-Peytavi et al., “Cutaneous lycopene and β-carotene levels measured by resonance Raman spectroscopy: High reliability and sensitivity to oral lactolycopene deprivation and supplementation,” Eur. J. Pharm. Biopharm., vol. 73, no. 1, pp. 187–194, 2009.spa
dc.relation.referencesJ. V. Freitas, F. S. G. Praça, M. V. L. B. Bentley, and L. R. Gaspar, “Trans-resveratrol and beta-carotene from sunscreens penetrate viable skin layers and reduce cutaneous penetration of UV-filters,” Int. J. Pharm., vol. 484, no. 1–2, pp. 131–137, 2015.spa
dc.relation.referencesE. J. Baek, C. V. Garcia, G. H. Shin, and J. T. Kim, “Improvement of thermal and UV-light stability of β-carotene-loaded nanoemulsions by water-soluble chitosan coating,” Int. J. Biol. Macromol., vol. 165, pp. 1156–1163, 2020.spa
dc.relation.referencesH. Phan-thi, P. Durand, M. Prost, E. Prost, and Y. Waché, “Effect of heat-processing on the antioxidant and prooxidant activities of b -carotene from natural and synthetic origins on red blood cells,” Food Chem., vol. 190, pp. 1137–1144, 2016.spa
dc.relation.referencesH. Sovová, M. Sajfrtová, M. Bártlová, and L. Opletal, “Near-critical extraction of pigments and oleoresin from stinging nettle leaves,” J. Supercrit. Fluids, vol. 30, no. 2, pp. 213–224, 2004.spa
dc.relation.referencesR. Li et al., “Combining Ability and Parent-Offspring Correlation of Maize (Zea may L.) Grain β-Carotene Content with a Complete Diallel,” J. Integr. Agric., vol. 12, no. 1, pp. 19–26, 2013.spa
dc.relation.referencesR. F. Martini and M. R. Wolf-Maciel, “A new methodology for mixture characterization and solvent screening for separation process application,” Comput. Chem. Eng., vol. 20, no. SUPPL.1, pp. 219–224, 1996.spa
dc.relation.referencesJ. L. Guil-Guerrero, M. M. Rebolloso-Fuentes, and M. E. Torija Isasa, “Fatty acids and carotenoids from Stinging Nettle (Urtica dioica L.),” J. Food Compos. Anal., vol. 16, no. 2, pp. 111–119, 2003.spa
dc.relation.referencesN. B. Ibrahim and Y. Noratiqah, “The microstructure and magnetic properties of yttrium iron garnet film prepared using water-alcohol solvents,” J. Magn. Magn. Mater., vol. 510, no. April, p. 166953, 2020.spa
dc.relation.referencesJ. Branisa, K. Jomova, M. Porubska, V. Kollar, M. Simunkova, and M. Valko, “Effect of drying methods on the content of natural pigments and antioxidant capacity in extracts from medicinal plants: A spectroscopic study,” Chem. Pap., vol. 71, no. 10, pp. 1993–2002, 2017.spa
dc.relation.referencesK. KŐszegi, G. Vatai, and E. BÉkÁssy-MolnÁr, “Comparison the soxhlet and supercritical fluid extraction of nettle root (Urtica dioica L.),” Period. Polytech. Chem. Eng., vol. 59, no. 3, pp. 168–173, 2015.spa
dc.relation.referencesA. E. Ince, S. Sahin, and G. Sumnu, “Comparison of microwave and ultrasound-assisted extraction techniques for leaching of phenolic compounds from nettle,” J. Food Sci. Technol., vol. 51, no. 10, pp. 2776–2782, 2014.spa
dc.relation.referencesI. Alibas, “Energy Consumption and Colour Characteristics of Nettle Leaves during Microwave, Vacuum and Convective Drying,” Biosyst. Eng., vol. 96, no. 4, pp. 495–502, 2007.spa
dc.relation.referencesI. Nencu, L. M. Popescu, V. Istudor, T. Costea, L. E. D. U. Ţ. U, and C. E. Gîrd, “The selection of thechnological parameters in order to obtain an extract with important antioxidant activity from stinging nettle leaves.,” vol. 65, 2017.spa
dc.relation.referencesM. Sajfrtová, H. Sovová, L. Opletal, and M. Bártlová, “Near-critical extraction of β-sitosterol and scopoletin from stinging nettle roots,” J. Supercrit. Fluids, 2005.spa
dc.relation.referencesW. Chen, Y. Liu, L. Song, M. Sommerfeld, and Q. Hu, “Automated accelerated solvent extraction method for total lipid analysis of microalgae,” Algal Res., vol. 51, no. August, p. 102080, 2020.spa
dc.relation.referencesL. Duan, L. L. Dou, L. Guo, P. Li, and E. H. Liu, “Comprehensive Evaluation of Deep Eutectic Solvents in Extraction of Bioactive Natural Products,” ACS Sustain. Chem. Eng., vol. 4, no. 4, pp. 2405–2411, 2016.spa
dc.relation.referencesI. Lee, Y. K. Oh, and J. I. Han, “Design optimization of hydrodynamic cavitation for effectual lipid extraction from wet microalgae,” J. Environ. Chem. Eng., vol. 7, no. 2, p. 102942, 2019.spa
dc.relation.referencesJ. Choi et al., “Hybrid reactor based on hydrodynamic cavitation, ozonation, and persulfate oxidation for oxalic acid decomposition during rare-earth extraction processes,” Ultrason. Sonochem., vol. 52, no. August 2018, pp. 326–335, 2019.spa
dc.relation.referencesK. E. Preece, N. Hooshyar, A. J. Krijgsman, P. J. Fryer, and N. J. Zuidam, “Intensification of protein extraction from soybean processing materials using hydrodynamic cavitation,” Innov. Food Sci. Emerg. Technol., vol. 41, pp. 47–55, 2017.spa
dc.relation.referencesM. Talebian, T. Abbasiasl, S. Niazi, and M. Ghorbani, “Direct and indirect thermal applications of hydrodynamic and acoustic cavitation : A review,” vol. 171, no. January, 2020.spa
dc.relation.referencesB. Lixin, Y. Jiuchun, Z. Zhijie, and M. Yuhang, “Cavitation in thin liquid layer : A review,” Ultrason. Sonochem., p. 105092, 2020.spa
dc.relation.referencesV. V. V. Cravotto Giancarlo, Cravotto Christian, “Ultrasound- and Hydrodynamic-Cavitation Assisted Extraction in food Processing,” Elsevier 1.22, pp. 359–366, 2021.spa
dc.relation.referencesV. Saharan, M. Badve, and A. Pandit, Degradation of Reactive Red 120 dye using Hydrodynamic cavitation, vol. 178. 2011.spa
dc.relation.referencesJ. Carpenter and V. Kumar, “Study of Cavity dynamics in a Hydrodynamic Cavitation Reactor,” vol. 1, no. 3, pp. 37–43, 2017.spa
dc.relation.referencesS. Đurović et al., “Chemical composition of stinging nettle leaves obtained by different analytical approaches,” J. Funct. Foods, vol. 32, pp. 18–26, 2017.spa
dc.relation.referencesA. Paulauskienė, Ž. Tarasevičienė, and V. Laukagalis, “Influence of harvesting time on the chemical composition of wild stinging nettle (Urtica dioica L.),” Plants, vol. 10, no. 4, 2021.spa
dc.relation.referencesM. Hojnik, M. Škerget, and Ž. Knez, “Isolation of chlorophylls from stinging nettle (Urtica dioica L.),” Sep. Purif. Technol., 2007.spa
dc.relation.referencesE. Food et al., “Scientific Opinion on the re-evaluation of chlorophylls (E 140(i)) as food additives,” EFSA J., vol. 13, no. 5, pp. 1–51, 2015.spa
dc.relation.referencesS. M. Nadakatti, J. H. Kim, and S. A. Stern, “Solubility of light gases in poly ( n-butyl methacrylate ) at elevated pressures,” J. Memb. Sci., vol. 108, pp. 279–291, 1995.spa
dc.relation.referencesS. Zeipiņa, I. Alsiņa, and L. Lepse, “Stinging nettle - the source of biologically active compounds as sustainable daily diet supplement,” Res. Rural Dev., vol. 1, pp. 34–38, 2014.spa
dc.relation.referencesD. Mihaylova et al., “Carotenoids, tocopherols, organic acids, carbohydrate and mineral content in different medicinal plant extracts,” Zeitschrift fur Naturforsch. - Sect. C J. Biosci., vol. 73, no. 11–12, pp. 439–448, 2018.spa
dc.rightsAtribución-NoComercial-SinDerivadas 2.5 Colombia
dc.rights.accessrightsinfo:eu-repo/semantics/openAccess
dc.rights.coarhttp://purl.org/coar/access_right/c_abf2
dc.rights.localAbierto (Texto Completo)spa
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/2.5/co/
dc.subject.keywordß-carotenesspa
dc.subject.keywordhydro-cavitationspa
dc.subject.keywordUrtica dioica Lspa
dc.subject.keywordchlorophyll Aspa
dc.subject.keywordchlorophyll Bspa
dc.subject.lembExtractionspa
dc.subject.lembStinging nettlespa
dc.subject.lembCavitationspa
dc.subject.proposalhydro-cavitationspa
dc.subject.proposalUrtica dioica Lspa
dc.subject.proposalchlorophyll Aspa
dc.subject.proposalchlorophyll Bspa
dc.subject.proposalß-carotenesspa
dc.titleObtaining nettle extracts (Urtica dioica L) by means of hydrocavitationspa
dc.typebachelor thesis
dc.type.categoryFormación de Recurso Humano para la Ctel: Trabajo de grado de Pregradospa
dc.type.coarhttp://purl.org/coar/resource_type/c_7a1f
dc.type.coarversionhttp://purl.org/coar/version/c_ab4af688f83e57aa
dc.type.driveinfo:eu-repo/semantics/bachelorThesis
dc.type.localTesis de pregradospa
dc.type.versioninfo:eu-repo/semantics/acceptedVersion

Archivos

Bloque original

Mostrando 1 - 3 de 3
Miniatura
Nombre:
2021estebanaguirre.pdf
Tamaño:
324.79 KB
Formato:
Adobe Portable Document Format
Descripción:
Trabajo de grado
Descargar
Miniatura
Nombre:
CARTA CRAI USTA Esteban Felipe Aguirre.pdf
Tamaño:
122.68 KB
Formato:
Adobe Portable Document Format
Descripción:
Carta facultad
Descargar
Miniatura
Nombre:
Carta_autorizacion_autoarchivo.pdf
Tamaño:
279.01 KB
Formato:
Adobe Portable Document Format
Descripción:
Carta autorizacion auto archivo
Descargar

Bloque de licencias

Mostrando 1 - 1 de 1
Miniatura
Nombre:
license.txt
Tamaño:
807 B
Formato:
Item-specific license agreed upon to submission
Descripción:
Descargar

Colecciones

Pregrado Ingeniería Mecánica