Synthesis and X-ray diffraction data of N1,N2-di(2-hydroxy) benzylidenbenzene-1,2-di-imine, C20H16N2O2

Vista sencilla de ítem
dc.contributor.authorCamargo, H. A.
dc.contributor.authorRosas, C. C.
dc.contributor.authorHenao, J. A.
dc.contributor.authorCastellanos, N. J.
dc.date.accessioned2019-07-05T21:10:40Z
dc.date.available2019-07-05T21:10:40Z
dc.date.issued2018-03-22
dc.description.abstractThe Schiff base N 1,N 2-di(2-hydroxy)benzylidenebenzene-1,2-di-imine was prepared from salicylaldehyde and 1,2-diaminobenzene by reflux in ethanol for 6 h obtaining an orange crystalline solid. The Schiff base solid was separated by filtration and washed with ethanol and ethylic ether, and finally, it was dried in a vacuum system for 2 h. The X-ray powder diffraction pattern for this new compound showed that the crystalline compound belongs to the monoclinic system and space group P21/c (No. 14) with refined unit-cell parameters a = 5.9672 (7) Å, b = 16.561 (1) Å, c = 16.337 (2) Å, β = 91.41° (1). The volume of the unit cell is V = 1614.1 (2) Å3.spa
dc.description.domainhttp://unidadinvestigacion.usta.edu.cospa
dc.format.mimetypeapplication/pdf
dc.identifier.doihttps://doi.org/10.1017/S0885715618000027spa
dc.identifier.urihttp://hdl.handle.net/11634/17481
dc.publisher.branchCRAI-USTA Bogotáspa
dc.relation.referencesAbo-Aly, M. M., Salem, A. M., Sayed, M. A., and Abdel Aziz, A. A. (2015) “Spectroscopic and structural studies of the Schiff base 3-methoxy-N-salicylidene-o-amino phenol complexes with some transition metal ions and their antibacterial, antifungal activities,” Spectrochimica Acta Part A: Mol. Biomol. Spectroscopy 136(Part B), 993–1000.spa
dc.relation.referencesAlsalim, T. A., Hadi, J. S., Ali, O. N., Abbo, H. S., and Titinchi, S. J. (2013) “Oxidation of benzoin catalyzed by oxovanadium (IV) Schiff base complexes,” Chem. Central J. 7, 1–8.spa
dc.relation.referencesAmer, S., El-Wakiel, N., and El-Ghamry, H. (2013) “Synthesis, spectral, antitumor and antimicrobial studies on Cu(II) complexes of purine and triazole Schiff base derivatives,” J. Mol. Structure 1049, 326–335.spa
dc.relation.referencesBell, D., Davies, M. R., Finney, F. J. L., Geen, G. R., Kincey, P. M., and Mann, I. S. (1996) “The effect of catalyst loading and donor ligands in the Mn(III) salen catalysed chiral epoxidation of chromenes: synthesis of BRL 55834,” Tetrahedron Lett. 37, 3895–3898.spa
dc.relation.referencesBoultif, A. and Loüer, D. (2004). “Indexing of powder diffraction patterns of low symmetry lattices by successive dichotomy method,” J. Appl. crystallogr. 37, 724–731.spa
dc.relation.referencesChen, L., Cheng, F., Jia, L., Wang, L., Wei, J., Zhang, J., Yao, L., Tang, N., and Wu, J. (2012) “Manganese(III) complexes of novel chiral unsymmetrical BINOL-Salen ligands: synthesis, characterization, and application in asymmetric epoxidation of olefins,” Appl. Catalysis A: General 415–416, 40–46.spa
dc.relation.referencesDas, P. and Linert, W. (2016) “Schiff base-derived homogeneous and heterogeneous palladium catalysts for the Suzuki–Miyaura reaction,” Coord. Chem. Rev. 311, 1–23.spa
dc.relation.referencesDe Rosa, M., Lamberti, M., Pellecchia, C., Scettri, A., Villano, R., and Soriente, A. (2006) “An efficient solvent free catalytic oxidation of sulfides to sulfoxides with hydrogen peroxide catalyzed by a binaphthylbridged Schiff base titanium complex,” Tetrahedron Lett. 47, 7233–7235.spa
dc.relation.referencesde Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern indexing,” J. Appl. Crystallogr. 1, 108–113.spa
dc.relation.referencesGhosh, P., Kumar, N., Mukhopadhyay, S. K., and Banerjee, P. (2016) “Sensitive and fluorescent Schiff base chemosensor for pico molar level fluoride detection: in vitro study and mimic of logic gate function,” Sensors Actuators B: Chemical 224, 899–906.spa
dc.relation.referencesGrzegorczyk, M., Kapturkiewicz, A., Sanjuan-Szklarz, F.W., and Nowacki, J. (2014) “Monomeric complexes of Re(CO)3+ ion with tridentate N∩N∩O − ligands – Schiff base derivatives of salicylic aldehyde,” Inorg. Chem. Commun. 46, 103–106.spa
dc.relation.referencesGupta, K. C. and Sutar, A. K. (2008) “Catalytic activities of Schiff base transition metal complexes,” Coord. Chem. Rev. 252, 1420–1450.spa
dc.relation.referencesJacobsen, E. N., Deng, L., Furukawa, Y., and Martínez, L. E. (1994) “Enantioselective catalytic epoxidation of cinnamate esters,” Tetrahedron 50, 4323–4334.spa
dc.relation.referencesLaugier, J. and Bochu, B. (2002). CHEKCELL. “LMGP-Suite Suite of Programs for the interpretation of X-ray. Experiments”, ENSP/ Laboratoire des Matériaux et du Génie Physique, BP 46. 38042 Saint Martin d’Hères, France. http://www.inpg.fr/LMGP and http://www. ccp14.ac.uk/tutorial/lmgp/.spa
dc.relation.referencesMiguell, A. D., Hubberd, C. R., and Stalick, J. K. (1981). “NBS* AIDS80: A FORTRAN program for crystallographic data evaluation,” National Bureau of Standards (USA), Tech. Note 1141.spa
dc.relation.referencesMondal, S., Mandal, S. M., Mondal, T. K., and Sinha, C. (2015) “Structural characterization of new Schiff bases of sulfamethoxazole and sulfathiazole, their antibacterial activity and docking computation with DHPS protein structure,” Spectrochimica Acta Part A: Mol. Biomol. Spectroscopy 150, 268–279.spa
dc.relation.referencesPioquinto-Mendoza, J. R., Rosas-Ortiz, J. A., Reyes-Martínez, R., Conelly-Espinosa, P., Toscano, R. A., Germán-Acacio, J. M., Avila-Sorrosa, A., Baldovino-Pantaleón, O., and Morales-Morales, D. (2015) “Synthesis, characterization and molecular structures of Ni(II) complexes derived from Schiff base pyridylimine ligands,” Inorganica Chimica Acta 438, 146–152.spa
dc.relation.referencesRachinger, W. A. (1948). “A correction for the α1 α2 doublet in the measurement of widths of X-ray diffraction lines,” J. Sci. Instrum. 25, 254.spa
dc.relation.referencesRosu, T., Pahontu, E., Maxim, C., Georgescu, R., Stanica, N., and Gulea, A. (2011) “Some new Cu(II) complexes containing an ON donor Schiff base: synthesis, characterization and antibacterial activity,” Polyhedron 30, 154–162.spa
dc.relation.referencesSarkar, N., Bhaumik, P. K., and Chattopadhyay, S. (2016) “Manganese(III) complexes with tetradentate salicylaldimine Shiff bases: synthesis, structure, self assembly and catalase activity,” Polyhedron 115, 37–46.spa
dc.rightsAtribución-NoComercial-CompartirIgual 2.5 Colombia
dc.rights.urihttp://creativecommons.org/licenses/by-nc-sa/2.5/co/
dc.subject.keywordTetradentate Schiff basespa
dc.subject.keywordX-ray powder diffractionspa
dc.subject.keywordBioactive compoundsspa
dc.titleSynthesis and X-ray diffraction data of N1,N2-di(2-hydroxy) benzylidenbenzene-1,2-di-imine, C20H16N2O2spa
dc.type.categoryGeneración de Nuevo Conocimiento: Artículos publicados en revistas especializadas - Electrónicosspa

Archivos

Bloque original

Mostrando 1 - 1 de 1
Miniatura
Nombre:
Synthesis and X-ray diffraction data of N1,N2-di(2-hydroxy) benzylidenbenzene-1,2-di-imine, C20H16N2O2.pdf
Tamaño:
122.07 KB
Formato:
Adobe Portable Document Format
Descripción:
Artículo SCOPUS
Descargar

Bloque de licencias

Mostrando 1 - 1 de 1
Miniatura
Nombre:
license.txt
Tamaño:
807 B
Formato:
Item-specific license agreed upon to submission
Descripción:
Descargar

Colecciones

Producción de Alto Impacto