Synthesis and X-ray diffraction data of N 1,N 2-di(2-hydroxy)benzylidenbenzene-1,2-di-imine, C20H16N2O2
dc.contributor.author | Castellanos, N. J | spa |
dc.contributor.author | Camargo, H. A | spa |
dc.contributor.author | Henao, J. A | spa |
dc.contributor.author | Rosas, C. C. | spa |
dc.coverage.campus | CRAI-USTA Bogotá | spa |
dc.date.accessioned | 2019-05-30T19:16:26Z | spa |
dc.date.available | 2019-05-30T19:16:26Z | spa |
dc.date.issued | 2018-03-22 | spa |
dc.description.abstract | The Schiff base N1,N2-di(2-hydroxy)benzylidenebenzene-1,2-di-imine was prepared from salicylaldehyde and 1,2-diaminobenzene by reflux in ethanol for 6 h obtaining an orange crystalline solid. The Schiff base solid was separated by filtration and washed with ethanol and ethylic ether, and finally, it was dried in a vacuum system for 2 h. The X-ray powder diffraction pattern for this new compound showed that the crystalline compound belongs to the monoclinic system and space group P21/c (No. 14) with refined unit-cell parameters a = 5.9672 (7) Å, b = 16.561 (1) Å, c = 16.337 (2) Å, β = 91.41° (1). The volume of the unit cell is V = 1614.1 (2) Å3. | spa |
dc.description.domain | http://unidadinvestigacion.usta.edu.co | spa |
dc.format.mimetype | application/pdf | spa |
dc.identifier.citation | Camargo, H. A., Rosas, C. C., Henao, J. A., & Castellanos, N. J. (2018). Synthesis and X-ray diffraction data of N 1,N 2-di(2-hydroxy)benzylidenbenzene-1,2-di-imine, C20H16N2O2 doi:10.1017/S0885715618000027 | spa |
dc.identifier.doi | https://doi.org/10.1017/S0885715618000027 | spa |
dc.identifier.uri | http://hdl.handle.net/11634/16987 | |
dc.relation.references | Abo-Aly, M. M., Salem, A. M., Sayed, M. A., and Abdel Aziz, A. A. (2015) “Spectroscopic and structural studies of the Schiff base 3-methoxy-N-salicylidene-o-amino phenol complexes with some transition metal ions and their antibacterial, antifungal activities,” Spectrochimica Acta Part A: Mol. Biomol. Spectroscopy 136(Part B), 993–1000. | spa |
dc.relation.references | Alsalim, T. A., Hadi, J. S., Ali, O. N., Abbo, H. S., and Titinchi, S. J. (2013) “Oxidation of benzoin catalyzed by oxovanadium (IV) Schiff base complexes,” Chem. Central J. 7, 1–8. | spa |
dc.relation.references | Bell, D., Davies, M. R., Finney, F. J. L., Geen, G. R., Kincey, P. M., and Mann, I. S. (1996) “The effect of catalyst loading and donor ligands in the Mn(III) salen catalysed chiral epoxidation of chromenes: synthesis of BRL 55834,” Tetrahedron Lett. 37, 3895–3898. | spa |
dc.relation.references | Chen, L., Cheng, F., Jia, L., Wang, L., Wei, J., Zhang, J., Yao, L., Tang, N., and Wu, J. (2012) “Manganese(III) complexes of novel chiral unsymmetrical BINOL-Salen ligands: synthesis, characterization, and application in asymmetric epoxidation of olefins,” Appl. Catalysis A: General 415–416, 40–46. | spa |
dc.relation.references | Das, P. and Linert, W. (2016) “Schiff base-derived homogeneous and heterogeneous palladium catalysts for the Suzuki–Miyaura reaction,” Coord. Chem. Rev. 311, 1–23. | spa |
dc.relation.references | De Rosa, M., Lamberti, M., Pellecchia, C., Scettri, A., Villano, R., and Soriente, A. (2006) “An efficient solvent free catalytic oxidation of sulfides to sulfoxides with hydrogen peroxide catalyzed by a binaphthylbridged Schiff base titanium complex,” Tetrahedron Lett. 47, 7233–7235. | spa |
dc.relation.references | Ghosh, P., Kumar, N., Mukhopadhyay, S. K., and Banerjee, P. (2016) “Sensitive and fluorescent Schiff base chemosensor for pico molar level fluoride detection: in vitro study and mimic of logic gate function,” Sensors Actuators B: Chemical 224, 899–906. | spa |
dc.relation.references | Gupta, K. C. and Sutar, A. K. (2008) “Catalytic activities of Schiff base transition metal complexes,” Coord. Chem. Rev. 252, 1420–1450. | spa |
dc.relation.references | Jacobsen, E. N., Deng, L., Furukawa, Y., and Martínez, L. E. (1994) “Enantioselective catalytic epoxidation of cinnamate esters,” Tetrahedron 50, 4323–4334. | spa |
dc.relation.references | Laugier, J. and Bochu, B. (2002). CHEKCELL. “LMGP-Suite Suite of Programs for the interpretation of X-ray. Experiments”, ENSP/ Laboratoire des Matériaux et du Génie Physique, BP 46. 38042 Saint Martin d’Hères, France. http://www.inpg.fr/LMGP and http://www. ccp14.ac.uk/tutorial/lmgp/. | spa |
dc.relation.references | Miguell, A. D., Hubberd, C. R., and Stalick, J. K. (1981). “NBS* AIDS80: A FORTRAN program for crystallographic data evaluation,” National Bureau of Standards (USA), Tech. Note 1141. | spa |
dc.relation.references | Pioquinto-Mendoza, J. R., Rosas-Ortiz, J. A., Reyes-Martínez, R., Conelly-Espinosa, P., Toscano, R. A., Germán-Acacio, J. M., Avila-Sorrosa, A., Baldovino-Pantaleón, O., and Morales-Morales, D. (2015) “Synthesis, characterization and molecular structures of Ni(II) complexes derived from Schiff base pyridylimine ligands,” Inorganica Chimica Acta 438, 146–152. | spa |
dc.relation.references | Rachinger, W. A. (1948). “A correction for the α1 α2 doublet in the measurement of widths of X-ray diffraction lines,” J. Sci. Instrum. 25, 254. | spa |
dc.relation.references | Rosu, T., Pahontu, E., Maxim, C., Georgescu, R., Stanica, N., and Gulea, A. (2011) “Some new Cu(II) complexes containing an ON donor Schiff base: synthesis, characterization and antibacterial activity,” Polyhedron 30, 154–162. | spa |
dc.relation.references | Sarkar, N., Bhaumik, P. K., and Chattopadhyay, S. (2016) “Manganese(III) complexes with tetradentate salicylaldimine Shiff bases: synthesis, structure, self assembly and catalase activity,” Polyhedron 115, 37–46. | spa |
dc.relation.references | Smith, G. S. and Snyder, R. L. (1979). “FN: A criterion for rating powder diffraction patterns and evaluating the reliability of powder-pattern indexing,” J. Appl. Crystallogr. 12, 60–65. | spa |
dc.relation.references | Valyaev, D. A., Lavigne, G., and Lugan, N. (2016) “Manganese organometallic compounds in homogeneous catalysis: past, present, and prospects,” Coordination Chem. Rev. 308(Part 2), 191–235. | spa |
dc.relation.references | Wang, W., Daran, J.-C., Poli, R., and Agustin, D. (2016) “OH-substituted tridentate ONO Schiff base ligands and related molybdenum(VI) complexes for solvent-free (ep)oxidation catalysis with TBHP as oxidant,” J. Mol. Catalysis A: Chemical 416, 117–126. | spa |
dc.relation.references | Xia, Q. H., Ge, H. Q., Ye, C. P., Liu, Z. M., and Su, K. X. (2005) “Advances in homogeneous and heterogeneous catalytic asymmetric epoxidation,” Chem. Rev. 105, 1603–1662. | spa |
dc.relation.references | Zoubi, W. A. (2013) “Biological activities of Schiff bases and their complexes: a review of recent works,” Int. J. Organic Chem. 3(3), 24. | spa |
dc.rights | Atribución-NoComercial-CompartirIgual 2.5 Colombia | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-sa/2.5/co/ | * |
dc.subject.keyword | Tetradentate Schiff base | spa |
dc.subject.keyword | X-ray powder diffraction | spa |
dc.subject.keyword | Bioactive compounds | spa |
dc.title | Synthesis and X-ray diffraction data of N 1,N 2-di(2-hydroxy)benzylidenbenzene-1,2-di-imine, C20H16N2O2 | spa |
dc.type.category | Generación de Nuevo Conocimiento: Artículos publicados en revistas especializadas - Electrónicos | spa |
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