Synthesis and X-ray diffraction data of dichlorodioxido (4,4-dimethoxycarbonyl-2,2′ -bipyridyl) molybdenum(VI)
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2014-03
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Abstract
The dichlorodioxido(4,4′
-dimethoxycarbonyl-2,2′
-bipyridyl)molybdenum(VI) complex was prepared
from molybdenum(VI) dichloride dioxide and 4,4-dimethoxycarbonyl-2,2-bipyridyl in CH2Cl2
obtaining a clear green solution. The molybdenum complex was separated by precipitation with
ethyl ether. The XRPD pattern for the new compound showed that the crystalline compound belongs
to the monoclinic space group P21/c (No 14) with refined unit-cell parameters a = 12.104(1) Å, b =
14.933 (2) Å, c = 11.010 (2) Å and ß = 115.409° (9). The volume of the unit cell is V = 1797.6 (3) Å3.
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